火焰原子吸收法测定高铁闪锌矿中低含量钢

doi:１０．３９６９／ｊ．ｉｓｓｎ．１００９－０４７９．２０２１．０３．００５

昆明冶金高等专科学校学报 ›› 2021, Vol. 37 ›› Issue (3): 26-.DOI: １０．３９６９／ｊ．ｉｓｓｎ．１００９－０４７９．２０２１．０３．００５

火焰原子吸收法测定高铁闪锌矿中低含量钢

李理¹，王锦亮²，宁门翠¹，彭莉¹，吴文彬¹

(1.昆明冶金高等专科学校环境与化工学院，云南昆明 650033;2.云锡集团文山锌钢冶炼有限公司，云南马关663701)

收稿日期:2021-02-26 出版日期:2021-06-13 发布日期:2023-12-12
作者简介:李理（１９７９－），男，云南石屏人，副教授，工学硕士，主要从事环境检测与污染治理技术研究

Determination of Low Content Indium in High-Iron Sphalerite by Flame Atomic Absorption Method

LI Li¹，WANG Jinliang²，NING Mencui¹ ，PENG Li¹, WU Wenbin¹

(1. Faculty of Environmental and Chemical Engineering, Kunming Metallurgy College, Kunming 650033, China;2. Wenshan Zinc Indium Smelting Co. , Itd. of Yunnan Tin Group, Maguan 663701, Yunnan， China)

Received:2021-02-26 Online:2021-06-13 Published:2023-12-12

摘要/Abstract

摘要： 针对高铁闪锌矿组成复杂，对矿石中低含量的测定干扰因素多等特点，建立了火焰原子吸收法测定高铁闪锌矿中低含量的方法。方法检出限为0.001 pg/mL，试样质量浓度在0.01 ~10 g/m 范图内与吸光度值A呈线性关系，线性方程相关系数r=0.999 93，不同加标量样品的加标回收率在98.1%101.4%之间，不同含量样品测定结的相对标准偏差在0.34% ~0.84%之间，方法准确度和精密度均能够满足要求。

关键词: 火焰原子吸收法, 高铁闪锌矿, 铟, 测定方法

Abstract:

In view of the complex composition of high-iron sphalerite and many interference factors for thedetermination of low-content indium in the ore, a flame atomic absorption method was established to determine the low-content indium in high-iron sphalerite. The detection limit of the method is 0.001 ugmL, and the concentration of indium sample is in the range of 0.01 ~ 10 ug/ml. It represents a linearrelationship with the absorbance value A and the correlation coefficient of the linear equation is 0. 999 93.The recovery rate of different spiked samples is 98. 1% to 101. 4% , and the relative standard deviation ofthe determination results of different content samples is 0. 34% ~0. 84%. The accuracy and precision ofthe method can thus meet the requirements.

Key words: flame atomic absorption method, high-iron sphalerite: indium, analytical method

中图分类号:

O657.31

李理, 王锦亮, 宁门翠, 彭莉, 吴文彬. 火焰原子吸收法测定高铁闪锌矿中低含量钢[J]. 昆明冶金高等专科学校学报, 2021, 37(3): 26-.

LI Li, WANG Jinliang, NING Mencui , PENG Li, WU Wenbin. Determination of Low Content Indium in High-Iron Sphalerite by Flame Atomic Absorption Method [J]. Journal of Kunming Metallurgy College, 2021, 37(3): 26-.

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http://kmyzxb.magtech.com.cn/CN/Y2021/V37/I3/26

火焰原子吸收法测定高铁闪锌矿中低含量钢

Determination of Low Content Indium in High-Iron Sphalerite by Flame Atomic Absorption Method

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